ANALYTICAL REPORT. Attn: Richard Boelter

Transcription

1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Community Drive Suite South Burlington, VT 00 Tel: (0)0- TestAmerica Job ID: 00-- TestAmerica Sample Delivery Group: 00- Client For: ARCADIS U.S. Inc Massena Facility, Route East Chevrolet Road Massena, New York Attn: Richard Boelter Authorized for release by: //0 :: AM James Madison, Senior Project Manager (0)0- jim.madison@testamericainc.com Designee for Kathryn Kelly, Project Manager I (0)0- kathryn.kelly@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Client: ARCADIS U.S. Inc Table of Contents TestAmerica Job ID: 00-- SDG: 00- Cover Page Table of Contents Definitions/Glossary Case Narrative Detection Summary Client Sample Results Surrogate Summary QC Sample Results QC Association Summary Lab Chronicle Certification Summary Method Summary Sample Summary Chain of Custody Receipt Checklists Page of //0

3 Definitions/Glossary Client: ARCADIS U.S. Inc Qualifiers Air - GC Semi VOA Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. * Recovery or RPD exceeds control limits Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Job ID: 00-- SDG: 00- Page of //0

4 Case Narrative Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Job ID: 00-- Laboratory: Narrative CASE NARRATIVE Client: ARCADIS U.S. Inc Project: ARCADIS - Central Foundry Massena NY Report Number: 00-- With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. RECEIPT The samples were received on /0/0; the samples arrived in good condition, properly preserved and on ice. The temperature of the cooler at receipt was.º C. PCB IN AIR Samples AIR-0, AIR-0 and AIR-0 were analyzed for PCB in Air in accordance with TO-A. The samples were prepared on /0/0 and analyzed on /0/0. The analysis of blank spike sample LCS 00-/-B yielded marginally low recoveries for aroclors and 0. Insufficient sample remains for re-extraction. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Page of //0

5 Detection Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Client Sample ID: AIR-0 Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit D Method Prep Type Aroclor J ug/m PUF TO-A Client Sample ID: AIR-0 Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit D Method Prep Type Aroclor ug/m PUF TO-A Client Sample ID: AIR-0 Lab Sample ID: 00-- Analyte Result Qualifier RL MDL Unit D Method Prep Type Aroclor ug/m PUF TO-A This Detection Summary does not include radiochemical test results. Page of //0

6 Client: ARCADIS U.S. Inc Client Sample ID: AIR-0 Date Collected: /0/ 0: Date Received: /0/ :0 Sample Container: PUF Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: 00-- Analyzed Aroclor U * ug/m PUF /0/ :00 /0/ :0 Aroclor U Aroclor U Aroclor J Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U Surrogate %Recovery Qualifier Unit D ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ :0 Limits Analyzed DCB Decachlorobiphenyl - /0/ :00 /0/ :0 DCB Decachlorobiphenyl - /0/ :00 /0/ :0 Tetrachloro-m-xylene 0-0 /0/ :00 /0/ :0 Tetrachloro-m-xylene 0-0 /0/ :00 /0/ :0 Client Sample ID: AIR-0 Date Collected: /0/ 0: Date Received: /0/ :0 Sample Container: PUF Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier RL MDL Lab Sample ID: 00-- Analyzed Aroclor U * ug/m PUF /0/ :00 /0/ :0 Aroclor U Aroclor U Aroclor Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U Unit D ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ :0 Surrogate %Recovery Qualifier Limits Analyzed DCB Decachlorobiphenyl - /0/ :00 /0/ :0 DCB Decachlorobiphenyl 0 - /0/ :00 /0/ :0 Tetrachloro-m-xylene /0/ :00 /0/ :0 Tetrachloro-m-xylene 0-0 /0/ :00 /0/ :0 Client Sample ID: AIR-0 Date Collected: /0/ 0: Date Received: /0/ :0 Sample Container: PUF Lab Sample ID: 00-- Method: TO-A - Pesticides and PCBs in Ambient Air Analyte Result Qualifier RL MDL Unit D Analyzed Aroclor U * ug/m PUF /0/ :00 /0/ : Aroclor U ug/m PUF /0/ :00 /0/ : Aroclor U ug/m PUF /0/ :00 /0/ : Page of //0

7 Client: ARCADIS U.S. Inc Client Sample ID: AIR-0 Date Collected: /0/ 0: Date Received: /0/ :0 Sample Container: PUF Method: TO-A - Pesticides and PCBs in Ambient Air (Continued) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: 00-- Analyzed Aroclor ug/m PUF /0/ :00 /0/ : Aroclor U Aroclor U Aroclor U * Aroclor U Aroclor U Surrogate %Recovery Qualifier Unit D ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : ug/m PUF /0/ :00 /0/ : Limits Analyzed DCB Decachlorobiphenyl - /0/ :00 /0/ : DCB Decachlorobiphenyl - /0/ :00 /0/ : Tetrachloro-m-xylene 0-0 /0/ :00 /0/ : Tetrachloro-m-xylene 0-0 /0/ :00 /0/ : Page of //0

8 Surrogate Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Method: TO-A - Pesticides and PCBs in Ambient Air Prep Type: Percent Surrogate Recovery (Acceptance Limits) DCB DCB TCX TCX Lab Sample ID Client Sample ID (-) (-) (0-0) (0-0) 00-- AIR AIR AIR-0 LCS 00-/-B Lab Control Sample 0 MB 00-/-B Method Blank Surrogate Legend DCB = DCB Decachlorobiphenyl TCX = Tetrachloro-m-xylene Page of //0

9 Client: ARCADIS U.S. Inc Method: TO-A - Pesticides and PCBs in Ambient Air QC Sample Results TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID: MB 00-/-B Client Sample ID: Method Blank Prep Type: Analysis : Prep : MB MB Analyte Result Qualifier RL Aroclor- 0. U ug/m PUF /0/ :00 /0/ :0 Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor 0 Aroclor Aroclor Surrogate MDL Unit D Analyzed 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 0. U ug/m PUF /0/ :00 /0/ :0 MB %Recovery MB Qualifier Limits Analyzed DCB Decachlorobiphenyl - /0/ :00 /0/ :0 DCB Decachlorobiphenyl - /0/ :00 /0/ :0 Tetrachloro-m-xylene 0-0 /0/ :00 /0/ :0 Tetrachloro-m-xylene 0-0 /0/ :00 /0/ :0 Lab Sample ID: LCS 00-/-B Client Sample ID: Lab Control Sample Prep Type: Analysis : Prep : Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Aroclor * ug/m PUF - Aroclor * ug/m PUF - Limits Surrogate LCS %Recovery LCS Qualifier Limits DCB Decachlorobiphenyl - DCB Decachlorobiphenyl - Tetrachloro-m-xylene 0-0 Tetrachloro-m-xylene Page of //0

10 QC Association Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Air - GC Semi VOA Pre Prep : Lab Sample ID Client Sample ID Prep Type Matrix Method Prep 00-- AIR-0 Air PUF to Air 00-- AIR-0 Air PUF to Air 00-- AIR-0 Air PUF to Air LCS 00-/-B Lab Control Sample Air PUF to Air MB 00-/-B Method Blank Air PUF to Air Prep : Lab Sample ID Client Sample ID Prep Type Matrix Method Prep 00-- AIR-0 Air 0C 00-- AIR-0 Air 0C 00-- AIR-0 Air 0C LCS 00-/-B Lab Control Sample Air 0C MB 00-/-B Method Blank Air 0C Analysis : Lab Sample ID Client Sample ID Prep Type Matrix Method Prep 00-- AIR-0 Air TO-A 00-- AIR-0 Air TO-A 00-- AIR-0 Air TO-A LCS 00-/-B Lab Control Sample Air TO-A MB 00-/-B Method Blank Air TO-A Page of //0

11 Lab Chronicle Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Client Sample ID: AIR-0 Lab Sample ID: 00-- Date Collected: /0/ 0: Date Received: /0/ :0 Prep Type Type Method Run Dilution Factor or Analyzed Analyst Pre Prep PUF to Air /0/ : NML TAL BUR Number Prep 0C /0/ :00 NML TAL BUR Analysis TO-A /0/ :0 ELD TAL BUR Lab Client Sample ID: AIR-0 Lab Sample ID: 00-- Date Collected: /0/ 0: Date Received: /0/ :0 Prep Type Type Method Run Dilution Factor or Analyzed Analyst Pre Prep PUF to Air /0/ : NML TAL BUR Number Prep 0C /0/ :00 NML TAL BUR Analysis TO-A /0/ :0 ELD TAL BUR Client Sample ID: AIR-0 Lab Sample ID: 00-- Date Collected: /0/ 0: Date Received: /0/ :0 Prep Type Type Method Run Dilution Factor or Analyzed Analyst Pre Prep PUF to Air /0/ : NML TAL BUR Number Prep 0C /0/ :00 NML TAL BUR Analysis TO-A /0/ : ELD TAL BUR Lab Lab Laboratory References: TAL BUR =, 0 Community Drive, Suite, South Burlington, VT 00, TEL (0)0- Page of //0

12 Certification Summary Client: ARCADIS U.S. Inc TestAmerica Job ID: 00-- SDG: 00- Laboratory: The certifications listed below are applicable to this report. Authority Program EPA Region Certification ID Expiration Date New York NELAP 0-- Page of //0

13 Client: ARCADIS U.S. Inc Method Summary TestAmerica Job ID: 00-- SDG: 00- Method Method Description Protocol Laboratory TO-A Pesticides and PCBs in Ambient Air EPA TAL BUR Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL BUR =, 0 Community Drive, Suite, South Burlington, VT 00, TEL (0)0- Page of //0

14 Client: ARCADIS U.S. Inc Sample Summary TestAmerica Job ID: 00-- SDG: 00- Lab Sample ID Client Sample ID Matrix Collected Received 00-- AIR-0 Air /0/ 0: /0/ : AIR-0 Air /0/ 0: /0/ : AIR-0 Air /0/ 0: /0/ :0 Page of //0

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17 Login Sample Receipt Checklist Client: ARCADIS U.S. Inc Job Number: 00-- Login Number: List Number: Creator: Young, Joseph W Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. 0 Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. N/A N/A N/A N/A N/A SDG Number: 00- List Source: Lab does not accept radioactive samples..ºc IR GUN CF=0 Page of //0